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InChI:InChI=1/C8H16Cl2O/c9-5-1-3-7-11-8-4-2-6-10/h1-8H2
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The invention provides a 1,4-dichlorobut...
The present invention relates to novel e...
Group 5 and 6 metal chlorides such as Mo...
tetrahydrofuran
methanol
4-(methoxy)-1-chlorobutane
bis-(4-chlorobutyl)ether
Conditions | Yield |
---|---|
With
thionyl chloride;
Yield given. Multistep reaction;
1) ice-water bath, 10 min., 2) 120-140 deg C, overnight;
|
tetrahydrofuran
bis-(4-chlorobutyl)ether
Conditions | Yield |
---|---|
With
sulfuric acid; trichlorophosphate;
|
56% |
With
trichlorophosphate;
at 70 - 80 ℃;
for 9h;
|
55% |
With
sulfuric acid; trichlorophosphate;
at 80 - 100 ℃;
|
|
With
thionyl chloride; sulfuric acid;
at 100 - 110 ℃;
|
tetrahydrofuran
phosgene
4-Chloro-1-butanol
methanol
4-(4-phenylcarbonyloxybutoxy)butyl benzoate
6-oxa-undecanedinitrile
4-(4-acetoxybutoxy)butyl acetate
4-chlorobutyl bromide
CAS:1268137-13-8